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Caprolactam must be very carefully puri ed to exclude small concentrations of (1) ferric ions, which would catalyze the thermal oxidative degradation of polycaprolactam and (2) aldehydes and ketones, which would markedly increase the oxidizability of caprolactam The impurities in caprolactam may retard the rate of caprolactam polymerization as well as having a harmful effect on the properties of the polymer and ber In the vacuum depolymerization of nylon 6, a catalyst must be used because in the absence of a catalyst, by-products such as cyclic ole ns and nitrides may form, which affects the quality of the caprolactam obtained [3] The caprolactam obtained must meet the speci cations of permanganate number, volatile bases, hazen color, ultraviolet (UV) transmittance, solidi cation point, and turbidity, in order to be used alone or in combination with virgin caprolactam [25] Reported caprolactam puri cation methods include recrystallization, solvent extraction, and fractional distillation. winforms pdf 417 PDF - 417 C# Control - PDF - 417 barcode generator with free C# ...
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