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Caprolactam must be very carefully puri ed to exclude small concentrations of (1) ferric ions, which would catalyze the thermal oxidative degradation of polycaprolactam and (2) aldehydes and ketones, which would markedly increase the oxidizability of caprolactam The impurities in caprolactam may retard the rate of caprolactam polymerization as well as having a harmful effect on the properties of the polymer and ber In the vacuum depolymerization of nylon 6, a catalyst must be used because in the absence of a catalyst, by-products such as cyclic ole ns and nitrides may form, which affects the quality of the caprolactam obtained [3] The caprolactam obtained must meet the speci cations of permanganate number, volatile bases, hazen color, ultraviolet (UV) transmittance, solidi cation point, and turbidity, in order to be used alone or in combination with virgin caprolactam [25] Reported caprolactam puri cation methods include recrystallization, solvent extraction, and fractional distillation.

Table 14.1 The most common stigmatizing situations reported by US adults, in descending order of frequency. Comments from children As an adult, having a child make fun of you. A child coming up to you and saying something like, You re fat! Others making negative assumptions about you Other people having low expectations of you because of your weight. Having people assume you have emotional problems because you are overweight. Physical barriers Not being able to t into seats at restaurants, theatres and other public places. Not being able to nd clothes that t. Being stared at Being stared at in public. Groups of people pointing and laughing at you in public. Inappropriate comments from doctors Having a doctor make cruel remarks, ridicule you, or call you names. A doctor blaming unrelated physical problems on your weight. Nasty comments from family A spouse/partner calling you names because of your weight. A parent or other relative nagging you to lose weight. Nasty comments from others Having strangers suggest diets to you. Being offered fashion advice from strangers. Being avoided, excluded, ignored Being unable to get a date because of your size. Being singled out as a child by a teacher, school nurse, etc. because of your size.

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Increased risk of congestive Potential decreased heart failure (rosiglitazone myocardial infarction and pioglitazone) risk (pioglitazone) Increased risk of myocardial infarction (rosiglitazone) Increased risk of bone fractures Expensive Acarbose Neutral Gastrointestinal side-effects Modest glucose lowering action Expensive Meglitinide analogues Pramlintide Increase Loss Short duration Hypoglycaemia Expensive Given by injection Gastrointestinal side-effects Expensive Exenatide, liraglutide Loss Given by injection Gastrointestinal side-effects Expensive Insulin Increase (less with detemir) Cheap Powerful glucoselowering action Hypoglycaemia Given by injection

One solvent extraction technique involves membrane solvent extraction Ion-exchange resins have been shown to be effective in the puri cation of aqueous caprolactam solutions In one such process, the oily impurities are removed by extraction with organic solvents, followed after treatment with carbon at 60 80 C Cationic and anionic exchange resins are then used to complete the puri cation process Ion-exchange resins remove all ionic impurities as well as colloidal and oating particles, that is, alkali metal salts formed in permanganate treatment are removed during ion-exchange treatment Also the treatment of aqueous solutions of caprolactam with ion-exchange resins helps to remove the distillation residue Treatment of caprolactam with activated carbon helps to remove anionic and cationic impurities Impurities in caprolactam have also been destroyed by oxidation with ozone followed by distillation Ozonation treatment of waste caprolactam leaves no ionic impurities.

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<!DOCTYPE html PUBLIC -//W3C//DTD XHTML 1.0 Strict//EN http://www.w3.org/TR/xhtml1/DTD/xhtml1-strict.dtd > <html xmlns= http://www.w3.org/1999/xhtml xml:lang= en lang= en > <head> <title>Saying hello with style</title> <link rel= stylesheet type= text/css href= common.css /> </head> <body> <h1>Saying hello with style</h1> < php function helloWithStyle( $font, $size ) { echo <p style=\ font-family: $font; font-size: {$size}em;\ >Hello, world!</p> ; } helloWithStyle( Helvetica , 2 ); helloWithStyle( Times , 3 ); helloWithStyle( Courier , 1.5 ); > </body> </html>

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