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These schedules overlap sufficiently so that there is a tendency for short, medium, and long rates to move in the same direction most of the time, but no tendency at all for them to move by similar amounts Over the ninety Februaries covered by the data in Table 53, the one-year and the thirty-year rates have generally risen and fallen together Corporate oneyear and thirty-year yields moved in opposite directions during only seven of the years 1900 1975 Over the shorter period 1955 1989, US government one-year and thirty-year yields also moved in opposite directions in seven years The timing of lows and highs has usually been similar for rates on both long and short maturities There were, however, a few important exceptions The low rates for shorts came in 1939 1942, but the lows for longer maturities tended to appear about 1946 or even as late as 1950.

2-121

2-122

Parts Open It Up! Circuit at First Glance Step-by-Step Bending Choosing a Cool Control Layout Case Considerations Marking the Board Drilling Holes Painting Control Mounting Soldering Testing Reassembly Musicality 257 258 259 260 260 260 260 260 261 262 262 263 264 264.

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The high yields for every maturity in the first half of the century were in 1918 1922; in the second half, they were in 1980 1982 HIGH-GRADE NEW ISSUE YIELDS AND YIELD SPREADS The trend and level of the corporate bond market have been described throughout this chapter in terms of market yields of seasoned issues rather than new issue yields A review of the market, however, requires some chronicling of the yields of new issues Table 55, which presents a sampling of new issue yields of prime corporate bonds, is based on a selection of high-quality issues The yields, until 1946, are not necessarily representative and are not sufficiently numerous or uniform to provide an index of new issue yields From 1946 through 1989, however, they are based on comparable averages of Aa public utility long-term new issue yields derived from all important new issues in this category.

2-8c-1

The rate constants for these reactions are orders of magnitude greater than those for the corresponding reactions of the diacid or diester reactants (Table 2-8) The use of such reactants in a novel low-temperature polymerization technique called interfacial polymerization has been extensively studied [Morgan and Kwolek, 1959a,b; Nikonov and Savinov, 1977] Temperatures in the range 0 50 C are usually employed Polymerization of two reactants is carried out at the interface between two liquid phases, each containing one of the reactants (Fig 2-11) Polyamidation is performed at room temperature by placing an aqueous solution of the diamine on top of an organic phase containing the acid chloride The reactants diffuse to and undergo polymerization at the interface The polymer product precipitates and is continuously withdrawn in the form of a continuous lm or lament if it has suf cient mechanical strength.

Mechanically weak polymers that cannot be removed impede the transport of reactants to the reaction site and the polymerization rate decreases with time The polymerization rate is usually diffusion-controlled, since the rates of diffusion of reactants to the interface are slower than the rate of reaction of the two functional groups (This may not be the situation when reactions with small rate constants are employed) Interfacial polymerization is mechanistically different from the usual step polymerization in that the monomers diffusing to the interface will react only with polymer chain ends The reaction rates are so high that diacid chloride and diamine monomer molecules will react with the growing polymer chain ends before they can penetrate through the polymer lm to start the growth of new chains There is thus a strong tendency to produce highermolecular-weight polymer in the interfacial process compared to the usual processes.

The table shows the yield at the offering date of one or two of the lowestyielding prime large new issues of straight long-term corporate bonds.

Also, interfacial polymerization does not require overall bulk stoichiometry of the reactants in the two phases Stoichiometry automatically exists at the interface where polymerization proceeds There is always a supply of both reactants at the interface due to diffusion from the.

FIGURE C-10

Fig. 2-11 Interfacial polymerization; removal of polymer lm from the interface. From Morgan and Kwolek [1959 a,b] (by permission of Division of Chemical Education, American Chemical Society, Washington, DC and Wiley-Interscience, New York); an original photgraph, from which this gure was drawn, was kindly supplied by Dr. P. W. Morgan.

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